IUAP VI

IUAP VI

Content

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SAP ref.

B/07831/03

Promotor(s)

M. Waroquier

Description

IUAP VI - Du Prez

POD-Wetenschapsbeleid
P6/KUL/51

Attachments (ZAP restricted field)

IAP VI documents and contract.pdf

Project funding (ZAP restricted)

Promotore(n): M. Waroquier, V. Van Speybroeck

Financierende instantie: BELSPO

Data: 01/01/2007 to 31/12/2011

Bedrag: €550.000,00

Personeel: T. Verstraelen, W. Dewitte, M. Van Houteghem, S. Cottenier, M. Vandichel, S. Catak

Title: Functional Supramolecular Systems (FS2)

Project publications (A1)

M. Van Houteghem, A. Ghysels, T. Verstraelen, W. Poelmans, M. Waroquier, V. Van Speybroeck

Critical analysis of the accuracy of models predicting or extracting liquid structure information

Journal of Physical Chemistry B 118 (9), 2451–2470 (2014)

http://dx.doi.org/10.1021/jp411737s

Y-Y Liu, K. Leus, T. Bogaerts, K. Hemelsoet, E. Bruneel, V. Van Speybroeck, P. Van der Voort

Bimetallic–Organic Framework as a Zero-Leaching Catalyst in the Aerobic Oxidation of Cyclohexene

ChemCatChem 5 (12), 3657–3664 (2013)

http://dx.doi.org/10.1002/cctc.201300529

M. Vandichel, F. Vermoortele, S. Cottenie, D. De Vos, M. Waroquier, V. Van Speybroeck

Insight in the activity and diastereoselectivity of various Lewis acid catalysts for the citronellal cyclization

Journal of Catalysis 305, 118-129 (2013)

http://dx.doi.org/10.1016/j.jcat.2013.04.017

K. Leus, G. Vanhaelewyn, T. Bogaerts, Y-Y Liu, F. Esquivel, F. Callens, G.B. Marin, V. Van Speybroeck, H. Vrielinck, P. Van der Voort

Ti-functionalized NH2-MIL-47: an effective and stable epoxidation catalyst

Catalysis Today 208, 97-105 (2013)

http://dx.doi.org/10.1016/j.cattod.2012.09.037

I. Değirmenci, T. Furuncuoğlu, O. Karahan, V. Van Speybroeck, M. Waroquier, V. Aviyente

Origins of the Solvent Effect on the Propagation Kinetics of Acrylic Acid and Methacrylic Acid

Journal of Polymer Science Part A: Polymer Chemistry 51 (9), 2024–2034 (2013)

http://dx.doi.org/10.1002/pola.26589

Y-Y Liu, S. Couck, M. Vandichel, M. Grzywa, K. Leus, S. Biswas, D. Volkmer, J. Gascon, F. Kapteijn, J.F.M. Denayer, M. Waroquier, V. Van Speybroeck, P. Van der Voort

New V-IV-Based Metal-Organic Framework Having Framework Flexibility and High CO2 Adsorption Capacity

Inorganic Chemistry 52 (1), 113-120 (2013)

http://dx.doi.org/10.1021/ic301338a

V. Van Speybroeck, K. Hemelsoet, K. De Wispelaere, Q. Qian, J. Van der Mynsbrugge, B. De Sterck, B.M. Weckhuysen, M. Waroquier

Mechanistic Studies on Chabazite-Type Methanol-to-Olefin Catalysts: Insights from Time-Resolved UV/Vis Microspectroscopy Combined with Theoretical Simulations

ChemCatChem 5 (1), 173-184 (2013)

http://dx.doi.org/10.1002/cctc.201200580

K. Leus, S. Couck, M. Vandichel, G. Vanhaelewyn, Y-Y Liu, G.B. Marin, I. Van Driessche, D. Depla, M. Waroquier, V. Van Speybroeck, J.F.M. Denayer, P. Van der Voort

Synthesis, characterization and sorption properties of NH2-MIL-47

Physical Chemistry Chemical Physics (PCCP) 14, 15562–15570 (2012)

http://dx.doi.org/10.1039/C2CP42137B

A. Yıldırım, A. Konuklar, S. Catak, V. Van Speybroeck, M. Waroquier, I. Doğan, V. Aviyente

Solvent-Catalyzed Ring-Chain-Ring Tautomerization in Axially Chiral Compounds

Chemistry - A European Journal 18 (40), 12725-12732 (2012)

http://dx.doi.org/10.1002/chem.201200363

M. Vandichel, K. Leus, P. Van der Voort, M. Waroquier, V. Van Speybroeck

Mechanistic insight into the cyclohexene epoxidation with VO(acac)(2) and tert-butyl hydroperoxide

Journal of Catalysis 294, 1-18 (2012)

http://dx.doi.org/10.1016/j.jcat.2012.06.002

M. Van Houteghem, T. Verstraelen, A. Ghysels, L. Vanduyfhuys, M. Waroquier, V. Van Speybroeck

Analysis of the basis set superposition error in molecular dynamics of hydrogen-bonded liquids: application to methanol

Journal of Chemical Physics 137 (10), 104506 (2012)

http://dx.doi.org/10.1063/1.4749929

T. Verstraelen, P.W. Ayers, V. Van Speybroeck, M. Waroquier

The Conformational Sensitivity of Iterative Stockholder Partitioning Schemes

Chemical Physics Letters 545, 138-143 (2012)

http://dx.doi.org/10.1016/j.cplett.2012.07.028

J. Van der Mynsbrugge, M. Visur, U. Olsbye, P. Beato, M. Bjørgen, V. Van Speybroeck, S. Svelle

Methylation of benzene by methanol: single-site kinetics over H-ZSM-5 and H-beta zeolite catalysts

Journal of Catalysis 292, 201-212 (2012)

http://dx.doi.org/10.1016/j.jcat.2012.05.015

L. Vanduyfhuys, T. Verstraelen, M. Vandichel, M. Waroquier, V. Van Speybroeck

Ab initio parametrized force field for the flexible metal-organic framework MIL-53(Al)

Journal of Chemical Theory and Computation (JCTC) 8 (9), 3217-3231 (2012)

http://dx.doi.org/10.1021/ct300172m

A. Ghysels, M. Vandichel, T. Verstraelen, M. van der Veen, D. De Vos, M. Waroquier, V. Van Speybroeck

Host-guest and guest-guest interactions between xylene isomers confined in the MIL-47(V) pore system

Theoretical Chemistry Accounts 131 (7) 1234-1246 (2012)

http://dx.doi.org/10.1007/s00214-012-1234-7

F. Vermoortele, M. Vandichel, B. Van de Voorde, R. Ameloot, M. Waroquier, V. Van Speybroeck, D. De Vos

Electronic effects of linker substitution on Lewis acid catalysis with Metal-organic frameworks

Angewandte Chemie int. Ed. 51(20), 4887-4890 (2012)

http://dx.doi.org/10.1002/anie.201108565

B. Dogan, S. Catak, V. Van Speybroeck, M. Waroquier, V. Aviyente

Free radical polymerization of ethyl methacrylate and ethyl alpha-hydroxy methacrylate: A computational approach to the propagation kinetics

Polymer 53 (15), 3211-3219 (2012)

http://dx.doi.org/10.1016/j.polymer.2012.05.018

S. Mangelinckx, B. De Sterck, F. Colpaert, S. Catak, J. Jacobs, S. Rooryck, M. Waroquier, V. Van Speybroeck, N. De Kimpe

Diastereoselective aldol reaction of zincated 3-chloro-3-methyl-1- azaallylic anions as key-step in the synthesis of 1,2,3,4- tetrasubstituted 3-chloroazetidines

Journal of Organic Chemistry 77 (7), 3415–3425 (2012)

http://dx.doi.org/10.1021/jo300203t

S. Stankovic, H. Goossens, S. Catak, M. Tezcan, M. Waroquier, V. Van Speybroeck, M. D'Hooghe, N. De Kimpe

Solvent-controlled selective transformation of 2-Bromomethyl-2-methylaziridines to functionalized aziridines and azetidines

Journal of Organic Chemistry 77, 3181-3190 (2012)

http://dx.doi.org/10.1021/jo202637a

J. Van der Mynsbrugge, K. Hemelsoet, M. Vandichel, M. Waroquier, V. Van Speybroeck

Efficient Approach for the Computational Study of Alcohol and Nitrile Adsorption in H-ZSM-5

Journal of Physical Chemistry C 116 (9), 5499-5508 (2012)

http://dx.doi.org/10.1021/jp2123828

T. Verstraelen, E. Pauwels, F. De Proft, V. Van Speybroeck, P. Geerlings, M. Waroquier

Assessment of atomic charge models for gas-phase computations on polypeptides

Journal of Chemical Theory and Computation (JCTC) 8 (2), 661-676 (2012)

http://dx.doi.org/10.1021/ct200512e

K. Leus, M. Vandichel, Y-Y Liu, I. Muylaert, J. Musschoot, H. Vrielinck, F. Callens, G.B. Marin, C. Detavernier, Y.Z. Khimyak, M. Waroquier, V. Van Speybroeck, P. Van der Voort

The coordinatively saturated vanadium MIL-47 as a low leaching heterogeneous catalyst in the oxidation of cyclohexene

Journal of Catalysis 285 (1) 196-207 (2012)

http://dx.doi.org/10.1016/j.jcat.2011.09.014

H. Goossens, K. Vervisch, S. Catak, S. Stankovic, M. D'Hooghe, F. De Proft, P. Geerlings, N. De Kimpe, M. Waroquier, V. Van Speybroeck

Reactivity of Activated versus Nonactivated 2-(Bromomethyl)aziridines with respect to Sodium Methoxide: a Combined Computational and Experimental Study

Journal of Organic Chemistry 76 (21), 8698-8709 (2011)

http://dx.doi.org/10.1021/jo201255z

T. Furuncuoğlu, I. Değirmenci, V. Aviyente, C. Atilgan, B. De Sterck, V. Van Speybroeck, M. Waroquier

Controlling the Tacticity in the Polymerization of N-Isopropylacrylamide: a computational study

Polymer 52 (24), 5503 - 5512 (2011)

http://dx.doi.org/10.1016/j.polymer.2011.10.009

K. Hemelsoet, A. Ghysels, D. Mores, K. De Wispelaere, V. Van Speybroeck, B.M. Weckhuysen, M. Waroquier

Experimental and theoretical IR study of methanol and ethanol conversion over H-SAPO-34

Catalysis Today 177 (1), 12-24 (2011)

http://dx.doi.org/10.1016/j.cattod.2011.05.040

S. Catak, K. Hemelsoet, L. Hermosilla, M. Waroquier, V. Van Speybroeck

Competitive Reactions of Organophosphorus Radicals on Coke Surfaces

Chemistry - A European Journal 17 (43), 12027–12036 (2011)

http://dx.doi.org/10.1002/chem.201100712

E. Pauwels, J. Asher, M. Kaupp, M. Waroquier

Cluster or periodic, static or dynamic - the challenge of calculating the g tensor of the solid-state glycine radical

Physical Chemistry Chemical Physics (PCCP) 13 (41), 18638-18646 (2011)

http://dx.doi.org/10.1039/C1CP21452G

K. Hemelsoet, A. Nollet, V. Van Speybroeck, M. Waroquier

Theoretical simulations elucidate the role of naphthalenic species during methanol conversion within H-SAPO-34

Chemistry - A European Journal 17(3) 9083–9093 (2011)

http://dx.doi.org/10.1002/chem.201100920

J.A. Martens, J.W. Thybaut, J.F.M. Denayer, S. Pulinthanathu Sree, A. Aerts, M-F. Reyniers, V. Van Speybroeck, M. Waroquier, A. Buekenhoudt, I. Vankelecom, W. Buijs, J. Persoons, G.V. Baron, S. Bals, G. Van Tendeloo, G.B. Marin, P.A. Jacobs, C. Kirschhock

Catalytic and molecular separation properties of Zeogrids and Zeotiles

Catalysis Today 168, 17-27 (2011)

http://dx.doi.org/10.1016/j.cattod.2011.01.036

T. Verstraelen, P. Bultinck, V. Van Speybroeck, P.W. Ayers, D. Van Neck, M. Waroquier

The significance of parameters in charge equilibration models

Journal of Chemical Theory and Computation (JCTC) 7 (6), 1750-1764 (2011)

http://dx.doi.org/10.1021/ct200006e

B. De Moor, A. Ghysels, M-F. Reyniers, V. Van Speybroeck, M. Waroquier, G.B. Marin

Normal Mode Analysis in Zeolites: Toward an Efficient Calculation of Adsorption Entropies

Journal of Chemical Theory and Computation (JCTC) 7(4), 1090-1101 (2011)

http://dx.doi.org/10.1021/ct1005505

K. Hemelsoet, F. De Vleeschouwer, V. Van Speybroeck, F. De Proft, P. Geerlings, M. Waroquier

Validation of DFT-Based Methods for Predicting Qualitative Thermochemistry of Large Polyaromatics

ChemPhysChem 12(6), 1100-1108 (2011)

http://dx.doi.org/10.1002/cphc.201000788

M. Van Houteghem, T. Verstraelen, D. Van Neck, C. Kirschhock, J.A. Martens, M. Waroquier, V. Van Speybroeck

Atomic Velocity Projection Method: A New Analysis Method for Vibrational Spectra in Terms of Internal Coordinates for a Better Understanding of Zeolite Nanogrowth

Journal of Chemical Theory and Computation (JCTC) 7, 1045-1061 (2011)

http://dx.doi.org/10.1021/ct100538c

S. Stankovic, S. Catak, M. D'Hooghe, H. Goossens, K. Abbaspour Tehrani, P. Bogaert, M. Waroquier, V. Van Speybroeck, N. De Kimpe

Synthesis of 3-Methoxyazetidines via an Aziridine to Azetidine Rearrangement and Theoretical Rationalization of the Reaction Mechanism

Journal of Organic Chemistry 76 (7), 2157-2167 (2011)

http://dx.doi.org/10.1021/jo102555r

A. Depla, E. Verheyen, A. Verfeyken, M. Van Houteghem, K. Houthoofd, V. Van Speybroeck, M. Waroquier, C. Kirschhock, J.A. Martens

UV-Raman and 29Si NMR Spectroscopy Investigation of the Nature of Silicate Oligomers Formed by Acid Catalyzed Hydrolysis and Polycondensation of Tetramethylorthosilicate

Journal of Physical Chemistry C 115(22), 11077-11088 (2011)

http://dx.doi.org/10.1021/jp109901v

A. Depla, D. Lesthaeghe, T.S. van Erp, A. Aerts, K. Houthoofd, F. Fan, C. Li, V. Van Speybroeck, M. Waroquier, C. Kirschhock, J.A. Martens

29Si NMR and UV-Raman Investigation of Initial Oligomerization Reaction Pathways in Acid-Catalyzed Silica Sol-Gel Chemistry

Journal of Physical Chemistry C 115 (9), 3562–3571 (2011)

http://dx.doi.org/10.1021/jp109901v

V. Van Speybroeck, J. Van der Mynsbrugge, M. Vandichel, K. Hemelsoet, D. Lesthaeghe, A. Ghysels, G.B. Marin, M. Waroquier

First principle kinetic studies of zeolite-catalyzed methylation reactions

JACS (Journal of the American Chemical Society) 133 (4), 888–899 (2011)

http://dx.doi.org/10.1021/ja1073992

A. Ghysels, H. Lee Woodcock III, J.D. Larkin, B.T. Miller, Y. Shao, J. Kong, D. Van Neck, V. Van Speybroeck, M. Waroquier, B.R. Brooks

Efficient Calculation of QM/MM Frequencies with the Mobile Block Hessian

Journal of Chemical Theory and Computation (JCTC) 7 (2), 496–514 (2011)

http://dx.doi.org/10.1021/ct100473f

D. Lesthaeghe, J. Van der Mynsbrugge, M. Vandichel, M. Waroquier, V. Van Speybroeck

Full Theoretical Cycle for both Ethene and Propene Formation during Methanol-to-Olefin Conversion in H-ZSM-5

ChemCatChem 3 (1), 208-212 (2011)

http://dx.doi.org/10.1002/cctc.201000286

E. Pauwels, H. De Cooman, M. Waroquier, E.O. Hole, E. Sagstuen

On the identity of the radiation-induced stable alanine radical

Physical Chemistry Chemical Physics (PCCP) 12, 8733-8736 (2010)

http://dx.doi.org/10.1039/C004380J

S. Catak, M. D'Hooghe, T. Verstraelen, K. Hemelsoet, A. Van Nieuwenhove, H-J. Ha, M. Waroquier, N. De Kimpe, V. Van Speybroeck

Opposite Regiospecific Ring Opening of 2-(Cyanomethyl)aziridines by Hydrogen Bromide and Benzyl Bromide: Experimental Study and Theoretical Rationalization

Journal of Organic Chemistry 75 (13), 4530–4541 (2010)

http://dx.doi.org/10.1021/jo100687q

A. Ghysels, T. Verstraelen, K. Hemelsoet, M. Waroquier, V. Van Speybroeck

TAMkin: A Versatile Package for Vibrational Analysis and Chemical Kinetics

Journal of Chemical Information and Modeling (JCIM) 50 (9), 1736–1750 (2010)

http://dx.doi.org/10.1021/ci100099g

K. Leus, I. Muylaert, M. Vandichel, G.B. Marin, M. Waroquier, V. Van Speybroeck, P. Van der Voort

The remarkable catalytic activity of the saturated metal organic framework V-MIL-47 in the cyclohexeneoxidation

Chemical Communications 46, 5085-5087 (2010)

http://dx.doi.org/10.1039/C0CC01506G

M. Sabbe, M-F. Reyniers, M. Waroquier, G.B. Marin

Hydrogen Radical Additions to Unsaturated Hydrocarbons and the Reverse β-Scission Reactions: Modeling of Activation Energies and Pre-Exponential Factors

ChemPhysChem 11 (1), 195-210 (2010)

http://dx.doi.org/10.1002/cphc.200900509

B. De Sterck, R. Vaneerdeweg, F. Du Prez, M. Waroquier, V. Van Speybroeck

Solvent Effects on Free Radical Polymerization Reactions: The Influence of Water on the Propagation Rate of Acrylamide and Methacrylamide

Macromolecules 43 (2), 827–836 (2010)

http://dx.doi.org/10.1021/ma9018747

L. Hermosilla, S. Catak, V. Van Speybroeck, M. Waroquier, J. Vandenbergh, F. Motmans, P. Adriaensens, L. Lutsen, T. Cleij, D. Vanderzande

Kinetic and Mechanistic Study on p-Quinodimethane Formation in the Sulfinyl Precursor Route for the Polymerization of Poly(p-phenylenevinylene) (PPV)

Macromolecules 43 (18), 7424–7433 (2010)

http://dx.doi.org/10.1021/ma1013012

D.D. Claeys, T. Verstraelen, E. Pauwels, C.V. Stevens, M. Waroquier, V. Van Speybroeck

Conformational Sampling of Macrocyclic Alkenes Using a Kennard−Stone-Based Algorithm

Journal of Physical Chemistry A 114 (25), 6879–6887 (2010)

http://dx.doi.org/10.1021/jp1022778

I. Değirmenci, S. Eren, V. Aviyente, B. De Sterck, K. Hemelsoet, V. Van Speybroeck, M. Waroquier

Modeling the Solvent Effect on the Tacticity in the Free Radical Polymerization of Methyl Methacrylate

Macromolecules 43 (13), 5602–5610 (2010)

http://dx.doi.org/10.1021/ma100608g

V. Van Speybroeck, R. Gani, R.J. Meier

The calculation of thermodynamic properties of molecules

Chemical Society Reviews 39, 1764-1779 (2010)

http://dx.doi.org/10.1039/B809850F

K. Hemelsoet, F. Van Durme, V. Van Speybroeck, M-F. Reyniers, M. Waroquier

Bond Dissociation Energies of Organophosphorus Compounds: an Assessment of Contemporary Ab Initio Procedures

Journal of Physical Chemistry A 114 (8), 2864–2873 (2010)

http://dx.doi.org/10.1021/jp908502d

M. Sabbe, A.G. Vandeputte, M-F. Reyniers, M. Waroquier, G.B. Marin

Modeling the influence of resonance stabilization on the kinetics of hydrogen abstractions

Physical Chemistry Chemical Physics (PCCP) 12, 1278-1298 (2010)

http://dx.doi.org/10.1039/B919479G

S. Catak, M. D'Hooghe, N. De Kimpe, M. Waroquier, V. Van Speybroeck

Intramolecular π−π Stacking Interactions in 2-Substituted N,N-Dibenzylaziridinium Ions and Their Regioselectivity in Nucleophilic Ring-Opening Reactions

Journal of Organic Chemistry 75 (3), 885–896 (2010)

http://dx.doi.org/10.1021/jo902493w

E. Pauwels, R. Declerck, T. Verstraelen, B. De Sterck, C.W.M. Kay, V. Van Speybroeck, M. Waroquier

Influence of Protein Environment on the Electron Paramagnetic Resonance Properties of Flavoprotein Radicals: A QM/MM Study

Journal of Physical Chemistry B 114 (49), 16655–16665 (2010)

http://dx.doi.org/10.1021/jp109763t

M. Budesinsky, I. Cisarova, J. Podlaha, F. Borremans, J.C. Martins, M. Waroquier, E. Pauwels

Structures of cyclic dipeptides: an X-ray and computational study of cis- and trans-cyclo(Pip-Phe), cyclo(Pro-Phe) and their N-methyl derivatives

Acta Crystallographica Section B Structural Science B66, 662-677 (2010)

http://dx.doi.org/10.1107/S0108768110040243

D.D. Claeys, C.V. Stevens, B.I. Roman, P. Van De Caveye, M. Waroquier, V. Van Speybroeck

Experimental and computational study of the ring opening of tricyclic oxanorbornenes to polyhydro isoindole phosphonates

Organic & Biomolecular Chemistry 8, 3644-3654 (2010)

http://dx.doi.org/10.1039/C002926B

M. D'Hooghe, S. Catak, S. Stankovic, M. Waroquier, Y. Kim, H-J. Ha, V. Van Speybroeck, N. De Kimpe

Systematic Study of Halide-Induced Ring Opening of 2-Substituted Aziridinium Salts and Theoretical Rationalization of the Reaction Pathways

European Journal of Organic Chemistry 25, 4920-4931 (2010)

http://dx.doi.org/10.1002/ejoc.201000486

A. Ghysels, V. Van Speybroeck, E. Pauwels, S. Catak, B.R. Brooks, D. Van Neck, M. Waroquier

Comparative study of various normal mode analysis techniques based on partial Hessians

Journal of Computational Chemistry 31 (5), 994-1007 (2010)

http://dx.doi.org/10.1002/jcc.21386

M. Vandichel, D. Lesthaeghe, J. Van der Mynsbrugge, M. Waroquier, V. Van Speybroeck

Assembly of cyclic hydrocarbons from ethene and propene in acid zeolite catalysis to produce active catalytic sites for MTO conversion

Journal of Catalysis 271 (1), 67-78 (2010)

http://dx.doi.org/10.1016/j.jcat.2010.02.001

Project related conferences, workshops, meetings & stays

ACS Spring 2012 National Meeting & Exposition

Sat, 24/03/2012 to Thu, 29/03/2012

Participants: S. Catak

Visit to COK

Thu, 08/03/2012

Participants: L. Joos

Meeting at COK (C. Kirsschock)

Tue, 29/11/2011

Participants: L. Joos

Belgium Science Policy (Belspo)–Annual Meeting for Interuniversity Attraction Poles (IUAP)

Mon, 21/11/2011 to Tue, 22/11/2011

Participants: S. Catak, M. Waroquier, V. Van Speybroeck, M. Van Houteghem, M. Vandichel

Visit Oslo University

Wed, 16/11/2011 to Fri, 18/11/2011

Participants: V. Van Speybroeck, J. Van der Mynsbrugge, K. De Wispelaere

WATOC 2011

Sun, 17/07/2011 to Fri, 22/07/2011

Participants: S. Catak, A. Ghysels, J. Van der Mynsbrugge

Visit Oslo University

Tue, 15/02/2011 to Thu, 17/02/2011

Participants: V. Van Speybroeck, J. Van der Mynsbrugge

IAP meeting

Thu, 16/09/2010

Participants: V. Van Speybroeck

ACS Spring 2010 National Meeting & Exposition

Tue, 16/03/2010 to Thu, 25/03/2010

Participants: B. De Sterck, S. Catak

Molsim-2009

Sun, 04/01/2009 to Fri, 16/01/2009

Participants: M. Van Houteghem, A. Ghysels, M. Vandichel

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IUAP VI

Primary tabs

Content

SAP ref.

Promotor(s)

Description

Attachments (ZAP restricted field)

Project funding (ZAP restricted)

Project publications (A1)

Project related conferences, workshops, meetings & stays

Postscript First

Postscript Second

Postscript Third

Preface First

Preface Second

Preface Third